| Yield (wt%) |
---|
| 5-HMF | FF | Total |
---|
Maximuma | 18.6 | 9.3 | 27.9 |
Average in the recycling | 16.2 | 9.1 | 25.3 |
- In all cases: cooling temperature of the cold trap; − 196 °C, internal diameter of the connector; 5 mm, tip position; − 5 mm, system pressure; 10 hPa, processing temperature; 180 °C, processing duration; 30 min, sample loading; 1wt%, sample particle size; between 45 and 90 µm
- aData shown in Fig. 9